Novel AAO films and hollow nanostructures fabricated by ultra-high voltage hard anodization.
نویسندگان
چکیده
Novel anodic aluminium oxide (AAO) films and hollow nanostructures were synthesized via a simple electrochemical and chemical etching route; fluctuating nanotube growth inside AAO film fabricated under ultra-high voltage was considered to be the main reason for the formation of such new structures.
منابع مشابه
Study the Effect of Anodization Parameters on the Morphology of Anodic Aluminium Oxide Films
Anodic Aluminium Oxide (AAO) membranes were fabricated using a modified 2 step anodization process. The effect of varying anodization voltage, time and temperature of electrolyte on the morphology of the pores was studied. AFM measurements showed that the anodized samples contain ordered pores of 32 nm in diameter and were 40nm apart.
متن کاملFast anodization fabrication of AAO and barrier perforation process on ITO glass
Thin films of porous anodic aluminum oxide (AAO) on tin-doped indium oxide (ITO) substrates were fabricated through evaporation of a 1,000- to 2,000-nm-thick Al, followed by anodization with different durations, electrolytes, and pore widening. A faster method to obtain AAO on ITO substrates has been developed, which with 2.5 vol.% phosphoric acid at a voltage of 195 V at 269 K. It was found th...
متن کاملFabrication of oxide nanostructures on glass by aluminum anodization and sol–gel process
A novel process of fabricating various oxide nanostructures on glass substrates is described. Transparent porous alumina films ( 6–150 nm) were first formed in acid solutions by anodization of aluminum layers sputter-deposited on a glass plate coated with a tin-doped indium oxide film. The porous alumina structures after pore-widened were then used as a host or a template in a sol–gel process t...
متن کاملSelf-ordered anodic aluminum oxide formed by H2SO4 hard anodization.
The self-ordering of nanoporous anodic aluminum oxide (AAO) in the course of the hard anodization (HA) of aluminum in sulfuric acid (H2SO4) solutions at anodization voltages ranging from 27 to 80 V was investigated. Direct H2SO4-HA yielded AAOs with hexagonal pore arrays having interpore distances D(int) ranging from 72 to 145 nm. However, the AAOs were mechanically unstable and cracks formed a...
متن کاملAAO-assisted synthesis of highly ordered, large-scale TiO2 nanowire arrays via sputtering and atomic layer deposition
Highly ordered nanoporous anodic aluminum oxide (AAO) thin films were fabricated in oxalic acid under a constant voltage via a two-step anodization process. To investigate the high-aspect-ratio (7.5:1) filling process, both sputtering and atomic layer deposition (ALD) were used to form TiO2 nanowires. Field emission scanning electron microscopy and high-resolution transmission electron microsco...
متن کاملذخیره در منابع من
با ذخیره ی این منبع در منابع من، دسترسی به آن را برای استفاده های بعدی آسان تر کنید
برای دانلود متن کامل این مقاله و بیش از 32 میلیون مقاله دیگر ابتدا ثبت نام کنید
ثبت ناماگر عضو سایت هستید لطفا وارد حساب کاربری خود شوید
ورودعنوان ژورنال:
- Chemical communications
دوره 46 2 شماره
صفحات -
تاریخ انتشار 2010